STEPS IN CREATING A FORMULA

This is when you will start your journey of becoming an formulator. You will blend all the science you’ve learned with your creative influences. It’s how you can make your mark in the industry.

The following 6 steps will help you take your ideas and convert them into functioning products whether food, cosmetics, beverage or fragrances.

  • Define your product before getting started. What functions do you want your product to achieve for your ideal customer.

    Ask yourself a few questions:

    Who is your ideal consumer?

    What do they need?

    What do you want it to look like?

    What form do you want it to come in? Powder, Pre-Packaged, Bottled

    It’s always good find reference / similar products. Get samples, how does it look and feel?

  • Starting formulas can be found by searching Google patents or the USPTO.gov website to find formulas.

    You can also find our starting formulas HERE

    NOTE: Understanding how much of an ingredient to add to your formula can be perplexing.

    You will use the manufacturers posted range for the ingredient's usage.

  • Once you have picked your starting formula you will determine how much you want to start off with. Use our Formula Excel Sheets HERE.

    Once you have these things you will want to list out your specifications you want to test once you have finished your batch. Gather all of your raw materials/ingredients, equipment and start making your batch. Be sure to wear safety glasses.

  • Let’s go ahead and get this out of the way. You most likely will not get a perfect formula on your first batch. You will weigh or measure out your ingredients, mix them together as your defined procedure and heat & cool as is required. During your formulation process be writing detailed notes with dates and times and results/observations in your lab notebook. These will come in handy when you need to make iterations/changes for your future batches.

    Understanding how much of an ingredient to add to your formula can be perplexing.

    Start with at least two trial samples; one using the lowest amount, that would deliver your desired impact, and another using the highest amount or if you have no experience with the ingredients then you may want to add a third sample using an amount in the middle of the range. Let your samples stabilize and then check for desired performance or aesthetics. If a supplier does not give you a suggested starting rate then you might not want to work with that supplier.

  • Once you’ve completed step 4, making your batch, you will want to nail down it’s specifications. After letting to sample equilibrate to ambient/room temperature, take measurements like pH, viscosity, and see if you are within your ideal specification.

    Another step you will want to possibly do is weigh your batch to see how much water you lost during the heating and/or cooling phase. If you have lost more than a few % of water you will want to add water to make up the difference in your next formula variation.

    You also want to try the product out on yourself and see if your formula meets your satisfaction. After this step, you will want to perform stability testing.

  • After you’ve performed the necessary tests on your product and determined where quality could be improved, you’ll need to make adjustments to try and improve your formula. A trick of mine with experiments that has been the most helpful is observing the effect that every ingredient has on the final formula. Once you know what the ingredients do, you’ll know which ones to increase or decrease to improve your formula.

    It may take more than 10 revisions to achieve a formula that meets your needs.

    This is an artistic science. The more you formulate, the more you gain experience, the more you’ll find ingredients that you like and which ones you want to avoid. Just as I did, you’ll end up making products and formulas that are genuinely unique to you.

Notes:

  • Checking the formula:

    Once you have finished calculating the percentages you will then have to make the formula again following the your calculations. The formula isn’t likely to be perfect but you will have a starting point. I like to use an excel spreadsheet to do this but it is possible to calculate manually, in fact that is how I started. Using this approach is ideal for anhydrous products but can be applied to other types of formulation. The key is to ensure that you know your ingredients well and read the data sheets of potent ingredients such as preservatives and fragrances and use your knowledge to decide the safest way to proceed.

  • Note on restricted ingredients:

    Restricted ingredients are those that need to be in the formula at a specific range or dose. They are normally things like preservatives, essential oils and fragrances. They are restricted because using too much or two little could negatively impact a formula or be unsafe at particular levels.

    If you have a formulation that contains restricted ingredients (essential oils/preservatives) you may end up being over or under that recommended dose and will need to adjust. Say you have an emulsion with water and oil phases and the preservative is over or under the recommended amount you should then adjust it to the desired level. To make sure the overall formula is calculated to 100% you may want to adjust the water content.


  • You can’t put everything in a beaker, mix it, and achieve your end formulation. Ingredients are grouped into different “phases” based on the following factors:

    • Solubility (e.g., water-soluble ingredients are mixed first with water, oil-soluble ingredients are mixed first with oil, etc.)

    • Processing temperature (e.g., you don’t want to add temperature-sensitive ingredients at a hot temperature, you may have to melt some waxes, etc.)

    • Mixing factors (e.g., it’s better to disperse xanthan gum in a glycol before adding it to water so that it doesn’t clump in the water)

    As you become more familiar with different formula types, you’ll have an easier time understanding why certain ingredients are grouped together in processing instructions.

  • This is the column where you list out each ingredient by trade name or INCI or both.

  • Professional formulas should always start in percentages and then be converted to the required batch size (weight). Having your formula broken down in percentages allows you to make sure the ratios between your ingredients can be scaled up and down accurately and know how much of that ingredient is required. Knowing your formula by percentages helps you understand where a formula has perhaps gone wrong. For example, we know that for most people if glycerin is added at more than 3% it can feel sticky.

  • AMOUNT TO ADD (G)

    We use this column to determine how many grams of an ingredient we’re going to add depending on our batch size. In the example formula, we will make a 500 g batch size. If we are to add 1% of glycerin to a 500 g batch size, then we need to add 5 g of glycerin to the formula:

  • This column is how much you actually put in your formula as you’re making it. This is very important to keep track of while you’re making your batch so that if things go sideways, you can review what you did to make sure you didn’t accidentally add too little or too much of an ingredient.

    It can be kind of difficult to write things and take notes as you make your formulas, but it’s important to do. I try to pre-weigh everything in beakers, weigh boats, and weigh papers as much as I can so I have less to write when I’m actually putting everything together.

    EXAMPLE:
    Simply put, 1% is equivalent to 1g, 5% is equivalent to 5g. In all cases 100g is the same as 100%. If you want to make double the amount you would multiply each ingredient by two. If you want to make 300g you would multiply by three and so on. If you wanted to scale up the above formula to 250g then it is easy. You will simply multiply each ingredient by 2.5 as below:

    Cocoa Butter 26.00 x 2.5 = 65g

    Kokum Butter 9.00 x 2.5 = 22.5g

    Sunflower Oil 17.00 x 2.5 = 42.5g

    Rosehip Oil 32.00 x 2.5 = 80g

    Vitamin E 1.00 x 2.5 = 2.5g

    Beeswax 15.00 x 2.5 = 37.5g

    TOTAL 250g

  • q.s. stands for qauntum satis in Latin, which means the amount which is enough. When you “q.s.” an ingredient in a formula, it means you add the remaining amount of the q.s.’d ingredient in a formula. In most formulas, this will almost always be water. To calculate how much water you need to add in the example formula

  • Concentration is the final expression of the ratio of the amount of an ingredient to the amount of product.

    Concentrations of ingredients are reported (if they are reported at all) as percentages. More specifically, they’re reported as weight percentages.

    There are three common ways to report it: volume per volume (v/v), weight per volume (w/v), and weight per weight (w/w).

    Example:

    An alcohol based fragrance’s concentration is 70% - 92% alcohol, depending on the type of fragrance.

    There is a limit on ingredients as well. For example. A lactic acid serum.. The maximum permitted lactic acid concentration in skin products is: 10% at a pH ≥3.5 for consumer use. It is 10–30% or a pH between 3.0–3.5 for professional use.

  • To learn more about your formulation / manufacturing process click HERE.

  • Weight percent (w/w)

    w/w is used to report concentration. For this measurement, volume measurements are ignored regardless of if components are liquids and only the weights are used.

    Example:
    20 grams Shea butter.
    20 grams Jojoba oil
    20 grams Beeswax.
    35 grams of Sugar
    3 grams of Vitamin E oil
    2 grams of Essential oil

    The weight percent (w/w) of each ingredient is:
    20% Shea Butter w/w
    20% Jojoba Oil w/w
    20% Beeswax w/w
    35% Sugar w/w
    3% Vitamin E oil w/w
    2% Essential Oil w/w

  • Weight per volume (w/v)

    Example: Vegetable Stock

    If you have a single solution (water) that is dissolving several different solid ingredients (vegetables), then mass concentration, or weight per volume (w/v), might be used to denote the concentration.

    It’s difficult to accurately report mass concentrations of solutions because the density has to be taken into account.

    For example, let’s say you’re dissolving 400 g of diced celery x into 600 mL of water to make 1000 g of a final solution. Let’s also say that the density of the final solution is 0.98g/ml. The final mass concentration is not 40% of celery , but rather 39.2% w/v because it must be multiplied by the final density.

    If you find that it’s complicated to report mass concentration accurately, we use it because there are small amounts of solid compounds (vegetables) dissolved in water. Water’s density is about 1, and the small amounts of dissolved compounds (vegetables) are most likely not changing the density. You can use this to keep track of concentrations.

  • Volume per volume (v/v)

    Volume concentration, or volume per volume (v/v), is mainly used for solutions that are made up of liquids.

    If you have 20 mL of perfume that is made up of 20 mL water, 3mL of Rosemary oil, 1 mL of preservatives, and 1 mL of essential oil, the concentration of each ingredient would be 20% water v/v, 3% Rosemary oil v/v, 1% preservatives v/v and 1% essential oil v/v.

  • To tare a scale means to zero out the weight of whatever was already on the scale, such as a bowl, plate, or container.

WEIGHING YOUR INGREDIENTS

The first thing you should do is make the product as you normally would, but as you go along, you should weigh and make a record of that weight.

Start by selecting the ‘grams’ setting on your scale. If your formulation requires 1 cup of cocoa butter, then take a container and put it on the scale, “tare” to 0.00g (kg/lb/mg/mcg), then scoop out the ingredient as you normally would into the container and record that weight. Do this with each ingredient, regardless of whether it is liquid or solid. You will then end up with the weight equivalent for each ingredient.

Secondly, you need to calculate the total weight of your ingredients by simply adding them together.

Thirdly, to work out the percentage (the fraction out of a 100 total amount) of each ingredient, you will need to divide each ingredient with the total weight amount, in this case 232g, and then multiply by 100.

As you see in the example, I have rounded to the nearest whole number. Of course you can round to one or two decimal places depending on how close to the original weight amount you want to get.

Now, add each number in the percentage column and you will have a total of 100%.

CREATE A FORMULA HERE - MASTER FORMULA RECORD

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